Iron(I) phosphide CL spectrum, 15 keV e- beam, CSIRO 2022

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Measurement details

Description CL spectrum of Iron phosphide (var. Fe3P)
Reference CSIRO 2022
https://research.csiro.au/microbeam-lab/
Date measured 2022-04-06
Material Iron(I) phosphide [ Fe3P ]
Specimen temperature Ambient
Analysis technique Cathodoluminescence (CL)
Instrument JEOL 8530F
Probe 15 keV electron beam
Beam current 75.1 nA
Probe diameter 2 μm
Detector name OceanOptics QEPRO
Det. technology CCD, Si, Peltier cooled
Slit width 400 μm
Acquisition time 6.33 s
Channel count 1024
Wavelength range 199.467 … 970.586 nm
Intensity range -52.1 … 5579 counts
Integral 842679 counts
Data filter Savitzky-Golay, 4th order, ±15 channels

Specimen details

Name S-22-010 Mnz
Owner CSIRO
Type Mineral concentrate
Form Polished section, epoxy mount

Composition

Nominal composition of Iron(I) phosphide [ Fe3P ].
Element Atoms At% Wt%
Fe 3 75 84.4
P 1 25 15.6
Total 4 100 100